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Electrochemically driven tandem addition–cyclization: synthesis of thiadiazinanes and thiophosphonates
DOI: 10.1039/D5GC01831E, PaperHonghao Zhou, Yike Zhang, Liting Ma, Xiangyang Liu, Chun Zhang, Feifei Tong, Dandan Hu, Jun-Qi Zhang, Jianguo Yang
An iodine-catalyzed electrochemical strategy for the sustainable synthesis of 1,2,5-thiadiazinanes and thiophosphonates was developed. This strategy demonstrates excellent functional group tolerance, sustainability, and facile scale-up potential.
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Anaerobic digestion-derived digestate valorization: green chemistry innovations for resource recovery and reutilization
DOI: 10.1039/D5GC01053E, Tutorial ReviewSamuel Jacob, Debajyoti Kundu, Anjani Devi Chintagunta, Sampath Kumar N. S, Palas Samanta, Chandan Mahata, Sukhendu Dey, R. G. Shibirathna, Arun Barathi, Sunil Kumar, Zhiwu Wang, Gaurav Goel
Green chemistry approaches to digestate valorization support circular bioeconomy and advance UN sustainable development goals.
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Visible-light-driven photocatalytic depolymerization of post-consumer PET to terephthalic acid via cerium catalysis with batch-to-flow scalability
DOI: 10.1039/D5GC01218J, CommunicationYujian Pang, Xiqun Wu, Zhijie Li, Jie Sun, Zhenjiang Li, Jiang-Kai Qiu, Jian Wang, Canliang Ma, Kai Guo
The first report of a cerium trichloride photocatalyst enabling ambient visible-light PET depolymerization in batch and microfluidic systems.
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Selective oxidation of glucose–galactose syrup to gluconic and galactonic acids
DOI: 10.1039/D5GC01381J, Communication
Open Access 
  This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Joseph Install, Anže Zupanc, Seonyeong Kim, Wenjia Wang, Marianna Kemell, George W. Huber, Timo RepoOxidation of Greek yoghurt acid whey derived GGS syrup to gluconic and galactonic acids with solubility driven separation provides a route to high value bioproducts from dairy waste.
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Switching between α-alkenylation and α-alkylation of nitriles by coupling multiple electrochemical methods
DOI: 10.1039/D5GC01206F, CommunicationKai Li, Tong Li, Yupu Zhang, Hao Yang, Qi Sun, Zhiyong Wang
Switching between α-alkenylation and α-alkylation of nitriles was achieved by strategically coupling multiple electrochemical redox methods.
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Machine learning-guided optimization for ionic liquid-based polyethylene terephthalate waste recycling
DOI: 10.1039/D5GC01998B, Paper
Open Access   This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.Ji Gao, Wenbo Peng, Andres Galindo, Ethan Slaton, Jose Perez Martinez, Guanghui Lan, Zhaohui TongMachine learning-based ionic liquid design and reaction condition optimization towards unified economic and environmental performance indicators.
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Flash recovery of lithium from spent anode graphite by carbothermal shock and water leaching
DOI: 10.1039/D5GC00745C, PaperDuanmei Song, Beikai Zhang, Hongbiao Du, Jing Wu, Jiadong Yu, Jinhui Li
The global boom in electric vehicles has led to an alarming accumulation of lithium-ion battery waste.
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“On water” metal-free direct C–H amination and imination of olefins via tandem SNAr, click chemistry, and molecular nitrogen release
DOI: 10.1039/D5GC01076D, Paper
Open Access 
  This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Sudripet Sharma, Seyedesahar Miraghaee, Sachin HandaThe hydrophobic effect of water facilitates clean and sustainable tandem transformations involving SNAr, click, and nitrogen evolution reactions, leading to metal-free C–H amination chemistry.
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A “wave-riding” biocatalysis: an all-enzyme system for genuinely green and flexible manufacture of machine-washable dyed wool fabrics
DOI: 10.1039/D5GC01614B, PaperXinrui Zhang, Jun Wang, Man Zhou, Yuanyuan Yu, Ping Wang, Qiang Wang
An all-enzyme strategy based on a “wave-riding” enzymatic mechanism was developed to achieve genuinely green manufacture of machine-washable dyed wool fabrics.
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Electrochemical selective incorporation of SO2 to synthesize fused-ring framework compounds
DOI: 10.1039/D5GC01138H, PaperZhi-Long Lei, Dan Tan, Jin-Tao Qin, Xiu-Jin Meng, Fei-Hu Cui, Hai-Tao Tang, Ying-Ming Pan
This paper proposes a mild and effective electrochemical synthesis method. Through electrochemical oxidation and free radical cascade reactions, SO2 undergoes selective insertion, generating two different families of fused-ring framework compounds.
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Solvent-promoted catalyst-free aminolytic degradation for chemical recycling of single and mixed plastic wastes
DOI: 10.1039/D5GC01068C, Paper
Open Access   This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Kai Cheng, Yu-I. Hsu, Hiroshi UyamaSchematical illustration of this work: aminolytic degradation for chemical recycling of plastic wastes under mild and catalyst-free conditions.
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Direct nitrile electrosynthesis from amino acids on nickel oxyhydroxide
DOI: 10.1039/D5GC01194A, CommunicationXudong Liu, Zhe Chen, Tao Jiang, Wei Du, Can Lei, Xueting Cao, Shuangshuang Cha, Mengxin Qu, Xinchi Zhou, Ming Gong
A promising method of synthesizing functional nitriles from amino acids on α-Ni(OH)2 pre-catalysts through consecutive oxidative dehydrogenation and decarboxylation.
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Two-step continuous flow aerobic oxidation of cannabidiol to cannabinoquinone derivatives
DOI: 10.1039/D5GC01304F, PaperManuel Zielke, Christof Aellig, Dominique M. Roberge, Christopher A. Hone, C. Oliver Kappe
A two-step continuous flow synthesis using molecular oxygen to prepare cannabidiol quinone derivative, Etrinabdione, under sustainable conditions is reported.
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Soft glass interphase engineering for ultra-stable aluminum metal batteries
DOI: 10.1039/D5GC01118C, PaperShibin Zhang, Yan Xu, Danni Zhang, Lishun Bai, Yue Liu, Ying He, Feiyan Yu, Chengjun Liu, Sijie Li, Zhi Chang
An eco-friendly soft ZnP-H2Im glass protects Al metal by enabling uniform Al-ion transport and nucleation. Al-metal cells achieve >10 000 h of cycle life and retain 95% of their capacity after 200 cycles when assembled with organic cathodes.
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Visible-light-induced selenium-mediated cascade cyclization of 2-isocyanobenzonitriles with secondary amines to access indole-fused polycyclics
DOI: 10.1039/D5GC01245G, PaperDongping Xu, Lizhen Jin, Mengya Huang, Wu Zhang
Controllable synthesis of indolo[2,3-b]quinoxalines and imidazo[4,5-b]indoles was achieved through the cascade cyclization of 2-isocyanobenzonitriles with secondary amines. An intramolecular EDA complex triggered this photochemical radical process.
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Aerobic oxidation of a covalent organic framework facilitating photocatalytic CO2 reduction with water
DOI: 10.1039/D5GC01528F, PaperJiangqi Ning, Qing Niu, Zheyuan Liu, Liuyi Li
Aerobic oxidation of the azine linkage in covalent organic frameworks yields highly reactive species, facilitating photocatalytic reduction of CO2 under aerobic conditions.
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Highly selective, catalyst-free CO2 reduction in strong acid without alkali cations by a mechanical energy-induced triboelectric plasma-electrolytic system
DOI: 10.1039/D5GC00977D, CommunicationHui Hu, Nannan Liu, Qinglong Ru, Wei Jiang, Yongcui Yang, Kailan Ma, Lixiang Meng, Zuliang Du, Bao Zhang, Gang Cheng
A mechanical energy-driven hybrid triboelectric plasma-electrochemical system in strong acids was constructed to trigger CO2 reduction at room temperature and atmospheric pressure without catalysts or alkali cations.
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Multidimensional metabolic engineering of Yarrowia lipolytica for highly efficient biosynthesis of betulinic acid
DOI: 10.1039/D5GC01276G, PaperXiaoyan Li, Liangcheng Jiao, Guowei Zhao, Yunchong Li, Yunjun Yan, Jinyong Yan
Yarrowia lipolytica was engineered for high-level betulinic acid production via modular pathway and organelle engineering, precursor and redox optimization, metabolic rewiring, and 3 L fermentation using cost-effective carbon sources.
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Polymer monomers fabricated from biomass platform molecules over metal-free catalysts
DOI: 10.1039/D5GC01162K, PaperSiwei Xu, Nian Xiang, Jie He, Yang Li, Huankun Nie, Liang Huang, Chongbei Wu, Zehui Zhang
A biomass-derived carbon catalyst is reported to facilitate the synthesis of 2,5-furandicarboxylic acid and glycolic acid through the selective oxidation of 5-hydroxymethylfurfural and 1,3-dihydroxyacetone, respectively.
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Rational design of a cost-efficient and eco-friendly fluorinated ether for high-energy and long-lived Li-metal batteries
DOI: 10.1039/D5GC00474H, PaperNan Li, Xue Han, Xinke Cui, Longji Xu, Chenxi Liu, Qiao Han, Kai Xi, Zhenglong Xu, Xiaobing Dai, Chong Mao, Lewen Yang, Weijiang Xue
The rational design for a cost-efficient and eco-friendly fluorinated ether for high-energy and long-lived Li-metal batteries.
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